木瓜齐墩果酸和熊果酸等三萜酸类薄层色谱分离鉴别
作者:
作者单位:

作者简介:

通讯作者:

基金项目:

国家“十二五”科技支撑计划(2011BAI04B06)


Identification of Triterpene Acids Including Oleanolic Acid and Ursolic Acid in Fructus chaenomelis by Thin-layer Chromatography
Author:
Affiliation:

Fund Project:

  • 摘要
  • |
  • 图/表
  • |
  • 访问统计
  • |
  • 参考文献
  • |
  • 相似文献
  • |
  • 引证文献
  • |
  • 资源附件
    摘要:

    [摘要]目的 建立木瓜齐墩果酸、熊果酸等三萜酸薄层色谱分离鉴别方法。方法 将点于硅胶G板上的样〖JP2〗品点浸入1%碘二氯甲烷溶液中预处理,以环己烷-丙酮-乙酸乙酯-甲酸(9∶2∶1∶0.2)为展开剂。结果 木瓜中熊果酸、齐墩果酸以及3-O-乙酰熊果酸能够被很好地分离和检识。结论薄层色谱法简便、可靠,使木瓜鉴别更具客观性和专属性。

    Abstract:

    [Abstract]Objective To establish efficient methods for identifying triterpene acids, including oleanolic acid and ursolic acid, in Fructus chaenomelis by thin-layer chromatography (TLC). Methods The drops of samples on the plate of silica gel G were preprocessed with methylene dichloride solution containing 1% iodine, and then developed with the developer consisting of cyclohexane-acetone-acetic ether-methanoic acid (9∶2∶1∶0.2). Results Oleanolic acid, ursolic acid, and 3-O-acetyl ursolic acid in Fructus chaenomelis could be identified clearly. Conclusion TLC is simple and reliable, and it has specificity and objectivity for identifying Fructus chaenomelis.

    参考文献
    相似文献
    引证文献
引用本文

程菁菁,谢晓梅,张圣龙,葛晓郡,黄丽丹.木瓜齐墩果酸和熊果酸等三萜酸类薄层色谱分离鉴别[J].安徽中医药大学学报,2012,31(1):68-70

复制
分享
文章指标
  • 点击次数:
  • 下载次数:
历史
  • 收稿日期:
  • 最后修改日期:
  • 录用日期:
  • 在线发布日期: 2012-05-29